Dicyclohexylammonium (S)-2-azido-3-phenylpropanoate
نویسندگان
چکیده
منابع مشابه
Dicyclohexylammonium (S)-2-azido-3-phenylpropanoate
The asymmetric unit of the title compound, C(12)H(24)N(+)·C(9)H(8)N(3)O(2) (-), consists of two dicyclo-hexyl-ammonium cations linked to two (S)-2-azido-3-phenyl-propano-ate anions by four short N-H⋯O hydrogen bonds with N⋯O distances in the range 2.712 (3)-2.765 (3) Å. The dicyclo-hexyl-ammonium cations and the aryl and carboxyl-ate groups of the anion are related by a pseudo-inversion centre,...
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The administration of CycloSaligenyl 3'-azido-2',3'-dideoxythymidine monophosphate (CycloSal-AZTMP) to CEM cells resulted in a concentration- and time-dependent conversion to the 5'-monophosphate (AZTMP), 5'-diphosphate (AZTDP), and 5'-triphosphate (AZTTP) derivatives. High ratios of AZTMP/AZTTP were found in the CEM cell cultures treated with CycloSal-AZTMP. The intracellular T(1/2) of AZTTP i...
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In the title compound, C(14)H(19)N(3)O(4), the perhydro-pyran ring adopts a chair conformation. An intra-molecular C-H⋯O hydrogen bond generates an S(6) ring motif. In the crystal packing, mol-ecules are linked by O-H⋯O hydrogen bonds, forming infinite chains along [100].
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The synthesis of the title compound is described. Deprotection of Cis(N-Trityl-3-azido-4-Styryl)-2-azetidinone to Cis-(3-azido-4-styryl)-2-azetidinone was found to be accelerated by the special salt effect under acidic condition
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2012
ISSN: 1600-5368
DOI: 10.1107/s1600536812025536